Black Book Companion - State-Of-The-Art Improvised Munitions [dp,explosives] (Paladin, 1990).pdf - Chemistry - Bimbrownicus

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Contents

'Preface

, ,

. vn

l.ead Nitrate

l.ead Azide ..... .

li;M¢kap Primary EXi)losive

•

SlJ1fu1ic Acid

I ~losive "D"

•

• •

Black liook Compunion:

SflJle.o!.the .A rl fmprovised Munitions

Cop yr ig hl C 1995 b~ Paladin Press

""ch Nitl'ate

Process for RUX Manufac lure

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ISBN f) · S73M- 577-4

Pri h.co in Ihe United Sta ll's ofAmcrial

t\Jrnace

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Publi~ht!d by Pallid in P ress, "division o f

Pa bdilJ Enterpri~s. InC-. r .o . B<,.o; 13117,

Bould~r. C(l lp rado S0306. USA.

(303) 44) ·725{)

J1.)!drogen Azide

• •

:'Ethvle ne Gl ycol Dinitrate

• • • •

-PYnamites

. . . , . . . . .

- . . .

t1astable Impac t-Sensitive Explos,ive

COpper~slug Charge .. ... .

ShotsheU Antipersonn el Mille

,Canister Grenade , . . . . .

DirC(.1 inqu iries ;lnd/N (lfder~ 10 the above address.

All righL~ n:.~crvcd. Except for LlSC in ~ review, no

portion of this book muy be rcp rod uwd in Hny form

wi thout the c'\:pr~ss wrillen pcmlis~ion of !.he puhli~hcr.

•

• • •

•

'(Canister Grenade LaunehcT'

Counterlorce Charges ...

Del~cord 5S~gallon-drtIm Ch a r'ge

.Offensive Hand Grenade . . . . .

Nl'ith~'r the lIu th or nllr the publisher assumes

~.ny Icspon~ibilily f{)r the usc: or misuse of

info rma ti o n COnlairll~d ill thi~ book.

POison~fil1ed Hollowhead ;\mrn unilion

'- , .

- '"

_._------------

FOR INFORMATION PURPOSES ONLY

HC Smoke , . . . . . . . . . . . . .

Si mplified Compound De tu nato rs

fUming Sul flllic I\ c id (Ol e um)

Potassium Cyanide . . . . .

Hy drogen-<..ya nide Grenade

Chlorine Genemto l' ....

, 76

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, 7H

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. 84

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· 87

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· 9 1

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· 96

111

Preface

Appendix A: Amendments

Appendix B: Che micals

Appendix C: Primary and Secondary Explosive s

117

1:Jlack Book Companion is written to amend and add to

::tneinicmnation (;ovet'(~d in Bla ck Book. volumes 1, 2, and

1 3At can he used by itself or in conjunction with the Black

IJngks and other books of the same nallll'e. The authors

have compiled a mass of iofoMnatiun, added their own

'W~, and have organized it all into the easy~lo~use Hlack

•

~k ramulI.

We at G&T are constan tly on the lookout for new ideas

, !lIli<

•

We would greatJy appreciate receivin g any

Of' comments about our work. Please kee p a copy

. a s we will not rn! able to retul1l anything sent

' lo

.... ; .

~nd correspondence to:

G&:r

BI;lck, Iwok Comptmion

% Paladin P ress

:p.o. Box 1307

Boulder, CO 8030()

,,,'

vii

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FOR INl"'ORMATION PURPOSES ONLY

l .

•

SIX: I iOIl I

No. 40

LEAD NITRATE

Lead nitrale is u sed in the Olanufac tur-e oJ le ad azide,

';. ,and <,an be used as a s trong oxidi7.er.

warning

\1 ~

~TBRIALS

SOURCES

The pr'ocedures in thi.... manual, the inherent toxicity of

the matetials, and th e resulting end pruduct are exu-emely

dangeroUS. Whe never dealing: with high explosives and p o-

te ntially harmful chemicals, special pr'ecautions mus t be

followe d in accordance with industry standards for ex-

pe ri me ntation and produc tion. Failure to strictly follow

su c h i.ndustry sta ndaJ'Cls may resull in harm to life and

limb. FUl1hem10rc, the manufacture of the produc Ls in thi s

milnua] is illegal a nd V\.<ill result in stiff legal penalties 10

the offender .

Therefore, the autho r and publisher disclaim any liabili ty

from any damages 01' injuries of any type that a l'ead er 01'

user of inform atio n contained ""ithin this manual mayen·

counte r'- from the u se of said infunnation. Use this manua l

and a ny e nd produ c t 0 1' by-product al your own d sk. This

mam mi L'i for informarion purposes only!

, ,

II, ~.i.tric acid

teOid metal pieces, lead

$.hO l , or pellets

Spor1ing goods ou tlet,

small ie,a d SCr.'lP

, . Glass or (;eramic jal's

Field grade (Sec . I. NO.4)

•

••

Ii Gl;tss stirring rod

~ J"Jt@'t source

Hot p lat e, e tc.

Faper towel!'>

I I II'ROCEDURE

I I; 'l.i:nl jarhalffullwilh nilde

~Cid, Place jaron hal plate

I I ~4 heat gently (d o not

III' }:Jrio,g to simmer).

- I

, I

(I :¢A:tJTION: Acid will

. :Q.~$lJ'Oy dothing and bUnl

• 'I :skih.lfany is spilled, wash

~ 'ita,Way with a large

: :qqahtity of water,'Do Flot

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" , 'mhale fume",.

:-:

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FOR INFORMATION PURPOSES ONl.V

FOR INFORMATION P URPOSES ONLY

•

..iI. When metal no long el"

dissolves, take jarotT ofheat

a{l"d allow to cool. Lei it mM!

z. \<Vhen oUI:;ide of jar is

warrn 10 the lauch, s lowly

add lead pieces w hi,le

slil1'ing.

~t least 6 houl'S.

,', ' ,

.p~r. towel int~ a glass

coh'rune!' and dIscard

?;:: lJP,1'eac ted metal.

"The liquid can be u sed

lead azide, ori! can

is gone.

3. Continue to add metal

w hil e slining unlil no IlIOr'C

d issoh'Cs . lnc m'L"iC h e a t but

do Ilol "Uow liquid 10 boil .

COnlinue 10 add the le.td .

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5: Filter liquid thI"Ough

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FOR INFORMATION PURPOSES ONLY

FOR INFORMATION PURPOSBS ONI.\'

StX;ti on I

No. 41

'PROCEDURE

1..,pUt .2 cups of the lead-

l.EAD AZlDB

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nitrate solution in the Ix)wl

Le.ld azide is a po\o\."Criul primary explosive that is wcU

suit ed few improvised detonators because it is relatively

easy 10 make ilfld is the second mos t effet:live initialing

explosive for improvisal'ion (next to DDNP, Sec. I. No. 19,1.

However, lead azide is nul very flame-sensitive, especially

\\:hen compressed. Therefore, it is necess<uy to add to the

lead azide a small a mounl (a VI! 10 l/ul-inch layer) of another'

name-sensitive primary explosiv() or sugar-chlorate ignite r

mix 10 insure ignition.

and o\ldd a teas poon of the

so4ium hydroxide. Heat

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~~pt1y- (0 50-60 C.

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MATERIALS

SOURCES

Lead nill'ate

Improvised (Sec. l, No. 40)

or chemical supply store

Chemical supply or

phologmphy supply store

Sodium azide

" "

Sodium hydroxide

Clystal drain opener'

Dex trin or com s tarc h

Chemical supply or

bfJ'ocelY s tore

Large jar

Large Pyrex bowl

2 , tfCIyslllllin e le ad nitrate

is used, dUlItP- 40 grams of

the c ,)'stai in 2 ClipS of

walTl1 w;lIer.

Water

Paper towel

'Thermometer

C()nlai.m~r

Black Book Companion - State-Of-The-Art Improvised Munitions [dp,explosives] (Paladin, 1990).pdf

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