Widma.pdf

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13 C NMR: δ 141.22 (323),
134.96 (299), 129.05 (1000),
127.78 (990), 28.52 (448),
20.94 (264), 15.77 (478)
1 H NMR (CDCl 3 ): δ 7.22-
6.960 (4H, m), 2.606 (2H, q),
2.313 (3H, s), 1.216 (3H, t)
CH
EI MS:
27.0 2
39.0 4
41.0 1
50.0 1
51.0 4
52.0 1
53.0 1
58.0 1
59.0 1
62.0 1
63.0 2
65.0 4
77.0 8
78.0 3
79.0 5
89.0 1
91.0 8
92.0 1
102.0 1
103.0 5
104.0 2
105.0 100
106.0 9
115.0 2
117.0 2
119.0 3
120.0 28 (M)
121.0 3
Źródło widm: www.aist.go.jp/ RIODB/SDBS
1085750895.012.png 1085750895.013.png 1085750895.014.png
13 C NMR: δ 170.20 (450),
169.76 (510), 151.28 (560),
134.90 (924), 132.51 (1000),
126.17 (986), 124.01 (974),
122.26, (397), 20.99 (674)
1 H NMR (CDCl 3 ): δ 11 (1H, bs),
8.125 (1H, m), 7.624 (1H, m),
7.356 (1H, m), 7.142 (1H, m),
2.352 (3H, s)
EI MS:
15.0 2
28.0 1
38.0 1
39.0 5
42.0 1
43.0 42
44.0 1
53.0 1
63.0 3
64.0 4
65.0 4
81.0 1
92.0 19
119.0 0
120.0 100
121.0 17
122.0 1
138.0 70
139.0 5
163.0 1
180.0 5 (M)
CHO
1085750895.015.png 1085750895.001.png 1085750895.002.png
1 H NMR (CDCl 3 ): δ 11
(1H, bs), 7.806 (1H, d,
J=16.1Hz), 7.557 (2H, m),
7.42 (1H, m),
7.40 (2H, m),
6.465 (1H, d, J=16.1Hz)
13 C NMR: δ 172.76 (403),
147.11 (488), 134.11 (507),
130.74 (378), 128.97 (1000),
128.40 (970), 117.44 (408)
104.0 5
105.0 2
107.0 2
119.0 4
120.0 8
130.0 5
131.0 25
132.0 2
148.0 100 (M)
149.0 10
52.0 5
53.0 1
60.0 1
61.0 1
62.0 2
63.0 6
65.0 3
65.5 2
69.0 1
73.0 1
74.0 7
75.0 5
EI MS:
18.0 1
27.0 3
28.0 1
37.0 1
38.0 2
39.0 5
45.0 2
46.0 1
49.0 1
50.0 11
51.0 29
51.5 3
76.0 6
77.0 39
78.0 6
79.0 2
91.0 20
92.0 4
94.0 1
101.0 1
102.0 22
103.0 51
CHO
1085750895.003.png 1085750895.004.png 1085750895.005.png
1 H NMR (D 2 0): δ 3.015 (1H, t),
2.280 (1H, t), 1.906 (1H, m)
13 C NMR: δ 182.13 (141),
40.21 (844), 35.33 (956),
24.50 (1000)
EI MS:
17.0 1
18.0 6
26.0 1
27.0 4
28.0 12
29.0 3
30.0 100
31.0 2
39.0 2
40.0 1
41.0 9
42.0 8
43.0 14
44.0 9
45.0 2
55.0 1
56.0 4
57.0 1
69.0 1
84.0 4
85.0 11
86.0 1
103.0 5 (M)
CHON
1085750895.006.png 1085750895.007.png 1085750895.008.png
1 H NMR (D 2 0): δ 3.783
(1H, m), 2.46 (2H, m),
2.14 (2H, m)
13 C NMR: δ 178.60 (306),
174.97 (382), 55.26 (829),
31.99 (857), 27.33 (1000)
EI MS:
16.0 4
17.0 6
18.0 9
26.0 2
27.0 4
28.0 26
29.0 3
30.0 3
39.0 2
40.0 1
41.0 26
42.0 3
43.0 2
44.0 4
45.0 2
54.0 2
55.0 3
56.0 18
57.0 1
59.0 4
66.0 1
72.0 1
73.0 3
74.0 1
83.0 9
84.0 100
85.0 5
100.0 2
101.0 10
129.0 4
146 (M)
CHON
1085750895.009.png 1085750895.010.png 1085750895.011.png

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